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+\documentclass{report}
+\usepackage{rotating}
+\usepackage{german,times,multirow,array}
+\usepackage[latin1]{inputenc}
+\begin{document}
+
+\newcommand{\headrotate}[1]
+ {\makebox[5mm][c]{\begin{rotate}{60}#1\end{rotate}}}
+\begin{table}
+\caption{Anwendungsübersicht über verschiedene
+ Derivatisierungsreagenzien II}
+\setlength{\extrarowheight}{1pt}
+\begin{tabular}{|ll|*6{c}|}\hline
+& & \multicolumn{6}{c|}{\large\bfseries Substratklasse}\\
+\rule{0mm}{25mm} & & % Freihalten in Höhe der Legende
+\headrotate{Alkohole} &
+\headrotate{Amine} &
+\headrotate{Aminosäuren} &
+\headrotate{Carbonsäuren} &
+\headrotate{Hydroxylgruppen} &
+\headrotate{Phenole}
+\rule{2mm}{0mm} \\ % rechter Rand
+\hline
+\multirow{5}{5mm}{\begin{turn}{90}\large\bfseries Reagenz\end{turn}}
+& Bortrifluorid-Methanol-Komplex & & & x & & & \\
+& Chlortrimethylsilan & x & x & x & x & x & x \\
+& Dichlordimethylsilan & & & x & & & \\
+& Hexamethyldisiloxan & & & & & x & \\
+& N-Methyl-bis(trifluoracetamid) & x & x & & & & x \\
+\hline
+\end{tabular}
+\end{table}
+
+\end{document} \ No newline at end of file